Coatings for pipes

Diveng is actively engaged in supplying 3-layer coatings for pipes. Three layered coatings, also sometimes referred to as 3LPE/3LPP, consist of Fusion Bonded Epoxy, or FBE, adhesive and polyethylene or polypropylene. Our 3-layer coatings are used in pipes that transport oil & gas, water, and other fluids. 3LPE and 3LPP coatings help to protect pipes from corrosion, provide chemical resistance and significantly increase lifetime of the pipelines. In addition, 3-layer PE or PP coated pipes can withstand various temperatures, ranging from extreme cold to the temperatures of up to 80 degrees. Our products are CSA and ISO approved and are used by a wide range of pipe manufacturers, whose products are utilized by some of the largest oil and gas companies in the world.

Products:

Fusion Bonded Epoxy (FBE), EN 301A

FBE powder coating helps to increase corrosion resistance of the pipes and is used as the first layer in the 3-layer coating systems. Typical applications of the fusion bonded epoxy typically begin with the cleansing of the surface. The main goal at this stage is to degrease the surface and remove rust and any impurities from the surface of the pipe. After that, the pipes are heated, typically to the temperatures ranging from 180 to 240 degrees. The FBE powder is then sprayed on the pipes, usually using electrostatic application method. The charged powder evenly wraps the surface of the pipes and then turns into a solid coating, either from the residual heat or from heating the pipes again. FBE powder coatings have numerous advantages, including efficient application and limitation of waste, compared to alternative options.

Further information about EN 301A Fusion Bonded Epoxy can be found here.

Adhesive, L-5REN2

L-5REN2 is an adhesive that is usually used as a second layer in the 3-layer PE and PP coatings for pipes. The product can be supplied in powder or granule form, depending on the requirements of the customer. The main goal of the adhesive is to bond together the FBE, used as a ground coating and Polyethylene or Polypropylene, as a topcoat. L-5REN2 can be applied by flat die or crosshead extrusion. Exact extrusion conditions will depend on the type of the equipment used and the size of the pipe. Typical thickness for the adhesive is 0.3 mm or greater. L-5REN2 has an outstanding durability and long-term bonding strength.

Further information about L-5REN2 adhesive can be found here.

Polyethylene Coating, EJ-EN8

Polyethylene is often used as an anti-corrosion material in the two- or three-layer coating systems. EJ-EN8 is applied as a third coat to pipes that are used to transport gas, oil or water. EJ-EN8 can be supplied either in powder or granule form, depending on the requirement of the customer, as well as in black or other colours. The product is compatible with a wide range of products, but it is recommended to use it with EN-301A FBE and L-REN2 adhesive.

Further information about EJ-EN8 polyethylene coating can be found here.

What we offer

Three-layer coatings supplied by Diveng provide excellent corrosion resistance, improve expected lifetime of pipes, and can be adjusted to work in extreme temperatures. Our products comply with the CSA, DIN and ISO standards and are widely used by leading pipe manufacturing companies. All three layers supplied by Diveng are manufactured in developing countries, which allows us to offer a competitive solution to proactively compete with European and North American products, while fully complying with the international standards, which results in our products being used in many countries and approved by leading pipe manufacturers.

Technical information and properties of the 3-layer PE coating:

FBE Parameters
Typical Requirements
Testing method
EN 301A
Volatile-matter content (moisture). Loss in weight, %, maximum
0.5
2 h under 105 °С
0.45
Solidification heat, J/g, minimum
30
ISO 11357-5:1999
Complies
Glass-transition temperature, °С, minimum
100
ISO 11357-2:1999 10 °С/min, Тmg
110
Storage time under 25 °С and 65 % R.H., months, minimum
12
Complies
Adhesive Parameters
Typical Requirements
Testing method
L-5REN2
Melt flow index (190 °С/2.16 kg), g/10 min.
2-8
ISO 1133:1997
2.5
Softening temperature, °С, min.
110
ISO 11359-3:1999 10°С/min, 10 N/см3orISO 306:2004(according to Vicat)
115
Yield strength under temperature 23 °С, MPa, minimum
10
ISO 527-2:2012 sample of type 1, 100 mm/min
18
Elongation at break under 23 °С, %, minimum
500
ISO 527-2:2012 sample of type 1, 100 mm/min
800
Brittle temperature, %, maximum
-70
dynamic method
≤-70
Water absorption after 1000 h of water exposure under temperature 80 °С, %, maximum
1
ISO 62:2008
0.1
Oxidation induction time under temperature 200 °С and flowing oxygen of 100 mm/min, min, minimum
20
ISO 11357-6:2002
28
Polyethylene Parameters
Typical Requirements
Testing method
EJ-EN8
Melt flow index, g/10 min
0.2-0.6
ISO 1133:1997 (190 °С, 2.16 kg)
0.5
Softening temperature, °С, minimum
115
ISO 11359-3:1999 10 °С/min, 10 N/сm2
118
Yield strength under temperature (20+3) °С, MPa, minimum
18
ISO 527-2:2012 sample of type 1, 100 mm/min
20
Elongation at break under temperature -45 °С, %, minimum
100
ISO 527-2:2012 sample of type 1, 50 mm/min
300
Stress cracking resistance under temperature 50 °С, h, minimum
5000
>5000
Brittle temperature, %, max.
-70
≤-70
Electrical volume resistivity, Ω cm, minimum
1014
5*1015
Penetration under temperature 60 °С, mm, maximum
0.2
0.15
Induction period of oxygen conduction under temperature 200 °С and flowing oxygen of 100 ml/min:
ISO 11357-6:2002
- initial composition, min, minimum;
80
150
- after 500 h of air aging under 120 °С, %, maximum change
50
30
- after 30 days of water exposure under temperature 95-100 °С, %, maximum change
50
32

Main characteristics of the finished three-layer coating (testing on cut template)

Characteristic
Temperature
Typical Requirements
Results of Divengs`s 3LPE coating
Impact strength, J/mm of thickness, minimum, under temperature
minus (45±3)°C
7 - 8
≥8
minus (40±3)°C
6 - 10
≥10
(25±10)°C
5 - 8
≥8
(50±5)°C
3
≥6
(60±3)°C
3 – 6
≥6
Adhesion, N/cm of width, minimum, under temperature
(25±10)°C
70 – 200
300
(40±3)°C
30
220
(60±3)°C
50 – 100
160
(80±5)°C
50 - 75
120
Adhesion decrease, % from initial value, maximum, after 1000 h of water testing under temperature
(20±5)°C
30
20
(40±3)°C
33
21
(60±3)°C
33
22
(80±3)°C
50
30
Area of coating cathodic disbandment, cm2, maximum, after 30 days of tests in 3% NaCl solution under temperature
(20±5)°C
3-5
Complies
(40±3)°C
10
(60±3)°C
7 - 10
(80±3)°C
15
Coating transient resistance in 3% NaCl solution under temperature (20±5) °С, Ω m2, minimum
-
1010
5*1012
Resistance to temperature cycling, number of cycles without scaling and cracking, minimum, under temperature
from minus (50±3)°C to (20±5)°C
10
≥10
from minus (60±3)°C to (20±5)°C
10
≥10
Resistance to cutting, residual thickness of coating on the test area, mm, minimum
-
1.5
2.0
Tensile strength at break of scaled coating, MPa, minimum, under temperature
(20±5)°C
12 - 18
23
(60±3)°C
10 - 15
18
Elongation at break of scaled coating, %, minimum, under temperature
minus (45±3)°C
100
280
minus (40±3)°C
100
300
(20±5)°C
200 - 350
700
Indentation resistance, mm, maximum, under test temperature
(20±5)°C
0,15 – 0.2
0.1
(40±5)°C
0.3
0.12
(60±3)°C
0,2 – 0.3
0.15
(80±3)°C
0.4
0.28
Coating adhesion under 23 °С after water exposure for 1000 h, N/cm, minimum
under 60 °С
50
250
under 80 °С
70 - 100
220
under 95 °С
100
200
Scaling area of coating under cathodic polarization after air exposure for 30 days, cm2, maximum
under 60 °С
10 - 15
Complies
under 80 °С
20
Heat aging resistance of coating polyethylene layer. Elongation at break after air exposure for 100 days, %, minimum
under 110 °С
300 - 400
600
under 120 °С
400
500
Decrease of elongation at break of scaled coating after 1000 h of air tests under (110±3) °С, in % of initial value, maximum
20 - 25
15
Change of melt flow index of polyethylene after air exposure under temperature (110±3) °С for 1000 h, in % of initial value, maximum
20 - 25
16
Elongation decrease after 500 h of exposure in artificial light weathering chamber under radiation intensity of 120 W/m2, %, maximum
30
20
Stress cracking resistance under temperature (50±3) °С, h, minimum
1000
≥2000
Degree of cure ∆Tg, °С, within limits
-3≤∆Tg≤+2
Complies
Shrinkage of coating polyethylene layer under temperature 140 °С, %, maximum
45
20